Shimadzu Corporation

FTIR Fourier Transform Infrared Spectrophotometer IRXross

The IRXross offers the high performance and easy operation that meets the demands of the pharmaceutical and chemical industries. IRXross provides an S/N ratio of 55,000:1, the highest in its class. It is also compliant with data integrity regulations required in the pharmaceutical field. On top of that, this model comes with the IR Pilot analysis support program, and as a result, accurate measurement results can be easily obtained even by users without extensive analysis experience.
 
  • Best-in-class S/N Ratio 55,000:1
  • Working range: 7800-350 cm-1 (standard)
  • Highly stable interferometer unit with Patented Dynamic Sequencing Mechanism
  • Easy maintenance with Moisture Drying feature in the patented device

FTIR Spectrometer IRXross

 
High-End Sensitivity for Countless Applications
 

The IRXross is a mid-level FTIR model that achieves high-end level S/N. It enables best-in-class low noise with P-P values of 55,000:1 for one minute of integration

 
Astoundingly Low Noise

The 100 %T line was obtained by successively measuring the background and sample values without placing a sample in the sample compartment. Excluding the peaks for water vapor and carbon dioxide, the noise level (P-P value) was within ±0.005 %T, which shows that it can acquire data with low noise.


                                                                                            IRXross 100 %T Line



55,000:1 S/N Enables Ultra-High-Sensitivity Measurements 
Using the IRXross with a single-reflection ATR attachment, an oil stain on paper was analyzed. Analyzing the sample directly without pretreatment would not result in good peaks, so n-hexane was applied to the stain area to extract the stain substances. Then a drop of the extract solution was placed on the ATR prism for analysis. The system is able to detect even the extremely weak 0.00023 absorbance signal with good sensitivity.




0,25 cm-1 Resolution Enables High-Resolution Measurements
N2O gas (500 ppm), considered an environmental problem as a greenhouse gas, was analyzed. Measuring the gas at high resolution shows the peaks near 2,230 cm-1 properly separated, whereas a resolution of 1.0 cm-1 only shows the peaks as two levels.



High-Speed Measurement Enables Faster Reaction Tracking
When tracking the curing reaction in UV curable resin, the data shows that the intensity of the peak at 1,635 cm-1 began decreasing 5.0 seconds after UV irradiation and the reaction was finished by 5.5 seconds.



Library Useful for Identification Testing and Contaminant Analysis

Approx. 12,000-spectra library
A wide variety of libraries, including Shimadzu’s unique libraries, reagents, polymers and more, is included standard. Searching with standard libraries provides high-quality search results without purchasing extra libraries
 
Complies Fully with Regulations
Humidity-Resistant Window Material Compatible with the Wavenumber Measurement Range Specified in Pharmacopoeia
Either a KBr or KRS-5 window can be selected. The KRS-5 window maintains humidity resistance up to 90 %RH (for temperatures up to 30 °C) and is compliant with pharmacopoeia wavenumber range requirements (350 to 7,800 cm-1).

Internal Dehumidifier (Optional) Ensures High Durability
This dehumidifier removes moisture from inside the interferometer electrolytically using a solid polymer electrolytic membrane. It maintains low humidity levels inside the interferometer without leaving the light source ON. Using the dehumidifier can reduce power consumption by about 90 % compared to leaving the light source illuminated.




IRXross Power Consumption during Startup (with Start Switch ON) and during Standby (with Start Switch OFF and Dehumidifier ON)


AIM-9000 Infrared Microscope


The AIM-9000 incorporates a bright, optimized optical system and a high-sensitivity MCT detector. In addition to enabling high-sensitivity measurement of micro samples, the system has been automated to ensure all steps involved in micro analysis can be performed quickly and easily.

  • Measurement of Microplastics and Use of Thermal-Damaged Plastics Library

    Microscopic plastic with a size of several μm to 5 mm or less is called microplastic. As a marine environmental problem that adversely affects coastlines and marine ecosystems, and consequently may potentially affect human health, microplastics have become a global issue in recent years. As early action is necessary to protect the global environment, various analytical devices are used to designate the sources of microplastics and study countermeasures.
     
    This article introduces measurement of microplastics with a size on the order of several mm and use of the Shimadzu thermal-damaged plastics library to identify the samples.
     
    Instrument: Shimadzu IRSpirit Fourier Transform Infrared Spectrophotometer (FTIR)
     

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